HCID 12343860, compound → HCID 20548759, compound

HRID 2058943Notes

Reaction equation

HRID 2058943 reaction equation
[ClH:1].[CH3:2][O:3][C:4]1[CH:5]=[C:6]([C:14]2[NH:15][NH:16][C:17]3[N:23]=[CH:22][CH:21]=[CH:20][C:18]=3[N:19]=2)[CH:7]=[C:8]([O:12][CH3:13])[C:9]=1[O:10][CH3:11]>C(O)(=O)C>[ClH:1].[CH3:13][O:12][C:8]1[CH:7]=[C:6]([C:14]2[N:15]([C:8](=[O:12])[CH3:7])[N:16]([C:4](=[O:3])[CH3:9])[C:17]3[N:23]=[CH:22][CH:21]=[CH:20][C:18]=3[N:19]=2)[CH:5]=[C:4]([O:3][CH3:2])[C:9]=1[O:10][CH3:11]

Participants

3

Reactant 1

HCID 12343860HCID 12343860, compound

Product 1

HCID 20548759HCID 20548759, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

12.0 g (0.032 mole) of 3-(3',4',5'-trimethoxyphenyl)-1,2-dihydropyrido[3,2-e]-as-triazine hydrochloride are boiled in 40 ml of glacial acetic acid for a short time. The reaction mixture is cooled and the separated product is filtered off.

Workup

  1. temperatureThe reaction mixture is cooled
  2. filtrationthe separated product is filtered off

Sources & evidence

ORD record
ord-a0b63771cc054712aa80c60b9cc81edb
Source dataset
uspto-grants-1982_03
Patent number
US04320127

Reaction notes

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