Nicotinoyl chloride → HCID 20548751, compound

HRID 2058944Notes

Reaction equation

HRID 2058944 reaction equation
[ClH:1].Cl.[CH2:3]([C:9]1[NH:10][NH:11][C:12]2[N:18]=[CH:17][CH:16]=[CH:15][C:13]=2[N:14]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[C:19]([Cl:27])(=[O:26])[C:20]1[CH:25]=[CH:24][CH:23]=[N:22][CH:21]=1>>[ClH:27].[ClH:1].[CH2:3]([C:9]1[NH:10][N:11]([C:19](=[O:26])[C:20]2[CH:25]=[CH:24][CH:23]=[N:22][CH:21]=2)[C:12]2[N:18]=[CH:17][CH:16]=[CH:15][C:13]=2[N:14]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

3

Reactant 2

HCID 82604Nicotinoyl chlorideHCID 20548756HCID 20548756, compound

Product 1

HCID 20548751HCID 20548751, compound

Procedure

12 g (0.04 mole) of 3-n-hexyl-1,2-dihydropyrido-[3,2-e]-as-triazine dihydrochloride are boiled with an excess of nicotinic chloride. The reaction mixture is cooled and the separated product is filtered off.

Workup

  1. temperatureThe reaction mixture is cooled
  2. filtrationthe separated product is filtered off

Sources & evidence

ORD record
ord-a4b8a856920741d6aeb13e11fbc5efc4
Source dataset
uspto-grants-1982_03
Patent number
US04320127

Reaction notes

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