Thionyl Chloride → HCID 88751475, compound

HRID 2058947Notes

Reaction equation

HRID 2058947 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([C:9]2[C:13]([C:14]([OH:16])=O)=[CH:12][S:11][N:10]=2)[CH:5]=[C:6]([SH:8])[CH:7]=1.S(Cl)([Cl:19])=O>>[Cl:1][C:2]1[CH:3]=[C:4]([C:9]2[C:13]([C:14]([Cl:19])=[O:16])=[CH:12][S:11][N:10]=2)[CH:5]=[C:6]([SH:8])[CH:7]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 20548813HCID 20548813, compound

Product 1

HCID 88751475HCID 88751475, compound

Procedure

50 g of the product of step (b) are dissolved in 500 ml of thionyl chloride and the mixture is held at 50° for 20 hours. The thionyl chloride is removed at 12 mm to obtain the heading compound.

Workup

  1. customThe thionyl chloride is removed at 12 mm
  2. customto obtain the heading compound

Sources & evidence

ORD record
ord-be2d0f71b0c74cb08320e5567f1314ac
Source dataset
uspto-grants-1982_03
Patent number
US04320133

Reaction notes

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