HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethanolamine → Ethyl (2-cyanoaziridin-1-yl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethanolamine | HCID 7618 | — |
| Reactant | HCID 20483660 | HCID 20483660 | — |
| Product | Ethyl (2-cyanoaziridin-1-yl)acetate | HCID 20483606 | 34% |
Reaction Steps
reaction of 2-bromo-3-(carbethoxymethylamino)-propionitrile hydrochloride (prepared by reacting 2,3-dibromopropionitrile with glycine ethyl ester; m.p. 70°-75° C.) with triethanolamine gives ethyl 2-cyano-1-aziridineacetate; b.p.0.1 : 88°-90° C.; yield 34% of theory;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04321194 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-75f3402201324efcb96ac1779725469a |
| Source note | uspto-grants-1982_03 |