HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 20154087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2-(4-Chlorophenoxy)-2-methylpropanoyl chloride | HCID 2781312 | — |
| Reactant | HCID 14202249 | HCID 14202249 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20154087 | HCID 20154087 | — |
Reaction Steps
6.75 g (25 mmol) of p-(1-adamantylacetyl)-phenol and 6 g (25.7 mmol) of 2-(p-chlorophenoxy)-isobutyric acid chloride was mixed with 60 ml of dry pyridine and kept at 40° C. for 4 hours. After addition of 40 ml of water a crystalline product was obtained which was sucked off, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04321268 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-38e106a69fc64f9db9a5dd5827e1c4b8 |
| Source note | uspto-grants-1982_03 |