Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 3-Pyridinecarbonyl chloride, hydrochloride (1:1) | HCID 88438 | — |
| Reactant | p-Cyclododecylphenol | HCID 19391072 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | p-Cyclododecylphenyl nicotinate | HCID 12940113 | — |
Reaction Steps
8 g (30.8 mmol) of p-cyclododecylphenol and 5.9 g (33.2 mmol) of nicotinic acid chloride hydrochloride was mixed with 140 ml of dry pyridine and kept at 30° C. for 15 hours. Subsequently, 42 ml of water was added slowly drop by drop, and the mixture cooled to 0° C. The crystallized precipitate was sucked off, freed from pyridine by washing with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04321268 |
|---|
| Source dataset | uspto-grants-1982_03 |
|---|
| ORD ID | ord-128822cdabe44e20a3731552ad027746 |
|---|
| Source note | uspto-grants-1982_03 |
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