HuagongsheHuagongshe Chemistry Print Report · For research reference only
Coumarin → Dihydrocoumarin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Coumarin | HCID 323 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Dihydrocoumarin | HCID 660 | — |
Reaction Steps
Coumarin (30 g, 0.205 moles) is reduced on the Parr apparatus in 200 ml ethyl acetate with 1 g platinum oxide at 40 psi. When the uptake ceased (ca. 1 hr.) the catalyst is removed by filtration and the filtrate evaporated to give a quantitate yield of dihydrocoumarin.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04321270 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-0084de63c87443a886a1c5f9620279f2 |
| Source note | uspto-grants-1982_03 |