HuagongsheHuagongshe Chemistry Print Report · For research reference only
o-Anisalacetone → 4-(2-Methoxyphenyl)butan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | o-Anisalacetone | HCID 139181 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 4-(2-Methoxyphenyl)butan-2-one | HCID 578563 | 45% |
Reaction Steps
The crude o-anisalacetone is hydrogenated (100 g/l liter of ethyl acetate and 1 g of platinum oxide) and then distilled to give 1.25 moles (45%) of 1-(o-methoxyphenyl)-3-butanone, bp 90°-110° C., 0.15 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04321270 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-bcb70724b9cd4fa78b8ae52079f446fc |
| Source note | uspto-grants-1982_03 |