HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 10922049, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | HCID 18410382 | HCID 18410382 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10922049 | HCID 10922049 | — |
| Product | HCID 20548168 | HCID 20548168 | — |
Reaction Steps
The above described cyanoethylated 1,2-diaminocyclohexane can then be reduced with hydrogen in the presence of ammonia, either in the presence and absence of a solvent, such as methyl alcohol, ethyl alcohol, isopropyl alcohol, etc. N-(2-cyanoethyl)-1,2-cyclohexanediamine, (2), can be reduced to give a triamine, N-(3-aminopropyl)-1,2-cyclohexanediamine, (4), while N,N'-di-(2-cyanoethyl)-1,2-diaminocyclohexane, (3), can be reduced to give tetramine, N,N'-di-(3-aminopropyl)-1,2-diaminocyclohexane, (5). ##STR18##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04321354 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-9b891d79c4594ce085c8b3d5d6aa4e58 |
| Source note | uspto-grants-1982_03 |