Water → HCID 13345543, compound

Participants

Reaction Steps

There were added 9 ml of n-propyl iodide to a mixture of 10 g of 8β-methoxy-carbonylergoline and 8.2 g of potassium carbonate in 500 ml of DMF. After 20 hours under stirring at room temperature, the reaction mixture was poured into water and the precipitate was filtered and crystallized from methanol to give 10 g of 6-n-propyl-8β-methoxycarbonylergoline melting at 202°-204° C.

Provenance & Evidence