Water → HCID 20548202, compound

Participants

Reaction Steps

To a solution of cyanuric chloride (38.0 g) in acetone (350 ml) was added dropwise a suspension of dodecylamine (18.5 g) in acetone (40 ml) at 10° C. After addition, the mixture was stirred for 4 hours at that temperature. The reaction mixture was poured into water (2 l) and extracted with ethyl acetate. The extract was dried over anhydrous sodium sulfate and ethyl acetate was distilled off. The resulting oil was purified with silica gel column chromatography (eluent=benzene:n-hexane=4:1) to afford N,N-bis-(2,4-dichloro-1,3,5-triazine-6-yl)-n-dodecylamine as white crystals melting at 50°-53° C.

Provenance & Evidence