HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20546023, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21953396 | HCID 21953396 | — |
| Product | HCID 20546023 | HCID 20546023 | 75% |
Reaction Steps
One hundred five grams (0.5 mol) of monoethyl phenylmalonate [JACS 74, 5897 (1952)] were refluxed with 119 gm of thionyl chloride in a water bath for 90 minutes, under stirring. The excess thionyl chloride was eliminated in vacuo, and the residue was distilled under reduced pressure (130° to 135° C./15 mm). An amount of 85.0 gm (75% of theory) of monoethyl phenylmalonate chloride was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04322418 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-37041e74e86f472a90905634a67d5ba9 |
| Source note | uspto-grants-1982_03 |