HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 12806745, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 4,5-Dichloroquinazoline | HCID 247911 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12806745 | HCID 12806745 | 46% |
Reaction Steps
A solution of 3.0 g of 4,5-dichloroquinazoline and 1.4 g of aniline in 20 ml of ethanol was heated, whereupon a violet reaction occurred and the reaction mixture solidified. After cooling, the solidified product was collected and recrystallized from ethanol to give 1.8 g (yield 46%) of the desired Compound No. 2 in the form of a pale yellow powder melting at 263°-267° C. (with decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04322420 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-372d0384dd0a4ccda59ee2b7da604dc4 |
| Source note | uspto-grants-1982_03 |