HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 2-[(1-butyl-2-methyl-1H-indol-3-yl)carbonyl]- → HCID 20523562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 2-[(1-butyl-2-methyl-1H-indol-3-yl)carbonyl]- | HCID 105559 | — |
| Reactant | N~1~,N~1~,N~3~,N~3~-Tetraethylbenzene-1,3-diamine | HCID 19382815 | — |
| Product | HCID 20523562 | HCID 20523562 | — |
Reaction Steps
In a manner similar to that described in part B above, 3.35 g (0.01 mole) of 2-[(1-n-butyl-2-methyl-3-indolyl)carbonyl]-benzoic acid and 2.42 g (0.011 mole) of N,N,N',N'-tetraethyl-m-phenylenediamine were interacted to obtain 3-[2,4-bis(diethylamino) phenyl]-3-(1-n-butyl-2-methyl-3-indolyl)phthalide (Formula III: R°=R1 =R2 =R3 =Y1 =H; R=CH2CH3 ; R4 =N(CH2CH3)2 ; R5 =CH3 ; R6 =(CH2)3CH3), as tan-colored crystals which melted at 78°-80° C. A toluene solution of the product spotted on silica gel developed an intense blue-black-colored image.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04322352 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-71de386989174a209feb0c8e7c0550f6 |
| Source note | uspto-grants-1982_03 |