HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalic Anhydride → HCID 12248790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalic Anhydride | HCID 6811 | — |
| Reactant | 2,5-Dimethyl-1H-indole | HCID 70965 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 12248790 | HCID 12248790 | 65.5% |
Reaction Steps
A mixture of 5.0 g (0.034 mole) of phthalic anhydride and 5.0 g (0.034 mole) of 2,5-dimethylindole in 30 ml of ethylene dichloride was refluxed for 20 hours, cooled and the separated solid filtered off and dried to obtain 3.8 g of 2-[(2,5-dimethyl-3-indolyl)carbonyl]benzoic acid (Formula VIII: R°=R1 =R2 =R3 =R6 =H; R5 =CH3 ; Y1 =CH3) as a pink-colored solid melting at 198°-200° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04322352 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-0b6b376f62f34916892964075ad9ec70 |
| Source note | uspto-grants-1982_03 |