HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 15572227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | Diisopropylaniline | HCID 32484 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15572227 | HCID 15572227 | — |
Reaction Steps
Dissolve 2,6-diisopropylaniline (53.1 g, 0.30 mol) and ethyl bromoacetate (55.1 g, 0.33 mol) in 200 ml DMF. After 72 hours, pour onto aqueous NaHCO3 and extract with hexane. Wash the hexane twice with water. Dry, concentrate and distill to obtain as a fraction b.p. 130°-145° C./0.1 mm N-ethoxycarbonylmethyl-(2,6-diisopropyl)aniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04322434 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-0826ba71fb6a4287ace3389dadde4140 |
| Source note | uspto-grants-1982_03 |