HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium tert-butoxide → HCID 13702609, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Reactant | HCID 70543745 | HCID 70543745 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13702609 | HCID 13702609 | 2,062.8% |
Reaction Steps
The procedure is carried out as in Example 1 (b) but with the use of 80.1 g (0.495 mol) of isobutylidene-3-aminomethylpyridine, 2.5 g (0.0223 mol) of potassium tert-butylate and 75 ml of toluene. After a reaction time of 1 hour at 30°-35° C., distillation yields 74.5 g (0.46 mol) of 3-pyridylmethylidene-isobutylamine; yield 93% of theory; b.p. 108° C./2×103Pa; nD20 =1.5198.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04322536 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-256c67fb114d46ca956cfe3d7e536726 |
| Source note | uspto-grants-1982_03 |