HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 11575461, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | HCID 11510103 | HCID 11510103 | — |
| Reactant | HCID 178418936 | HCID 178418936 | — |
| Product | HCID 11575461 | HCID 11575461 | — |
Reaction Steps
This material was prepared according to the procedure outlined above for 2-(N-imidazolyl)-7-hydroxy-3-(3,4,5-trimethoxybenzoyl)-6-methoxy-benzo[b]furan (entry 27, Table 1), above, except the 1,2,3-triazole was used as the nucleophile in place of imidazole. 1H NMR (300 MHz, CDCl3) δ 8.47(d, 1H, J=1.21 Hz), 7.75(d, 1H, J=1.20 Hz), 7.27(d, 1H, J=8.60 Hz), 7.18(d, 1H, J=8.66 Hz), 7.05(s, 2H, benzoyl Hs), 3.94 (s, 3H, OMe), 3.74(s, 6H, 2×OMe), 3.73(s, 3H, OMe).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08278290B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-359daba1d9f544ceb3ac5e3da37d305d |
| Source note | uspto-grants-2012_10 |