Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | HCID 59370483 | HCID 59370483 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 59370481 | HCID 59370481 | — |
Reaction Steps
To a solution of {2-[2-methyl-3-(methyloxy)phenyl]ethyl}formamide (Preparation 11; 1.93 g; 10.0 mmol) in formic acid (20 ml) was added paraformaldehyde (0.315 g; 10.5 mmol) and the resulting mixture was heated under reflux (100° C.) for 20 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08278324B2 |
|---|
| Source dataset | uspto-grants-2012_10 |
|---|
| ORD ID | ord-890aadfbbf724d83a0e8401bd6cbfbc4 |
|---|
| Source note | uspto-grants-2012_10 |
|---|
