HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 178468176, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 178468173 | HCID 178468173 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178468176 | HCID 178468176 | — |
Reaction Steps
A solution of trans-N-(4-ethoxycyclohexyl)phthalimide (D64, 16.35 g), hydrazine hydrate (12 mL) in ethanol (300 mL) and methanol (200 mL) was stirred at reflux for 3 hours. The solvent was removed to give a slurry, which was treated with diethyl ether and filtered. The filtrate was evaporated to afford the title compound as a viscous oil contaminated with ether (8.16 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08278328B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-ce96fe8c8a88477b80d9a5c9b2c90d83 |
| Source note | uspto-grants-2012_10 |