HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2060304Generated: November 1, 2026
o-Fluorobenzaldehyde → HCID 57924005, compound
https://huagongshe.com/reaction/2060304
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | o-Fluorobenzaldehyde | HCID 67970 | — |
| Reactant | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Reactant | Ethyl 2-oxo-3-phenylpropanoate | HCID 12292599 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57924005 | HCID 57924005 | — |
Reaction Steps
3-Imidazol-1-yl-propylamine (1 mmol) and 2-Fluoro-benzaldehyde (1 mmol) were added to ethanol (5 ml). After 30 min 2-Oxo-3-phenyl-propionic acid ethylester (1 mmol) was added. The reaction was heated to 50° C. and stirred for 24 h. After evaporation of the solvent the residue was purified with chromatographic methods.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08278345B2 |
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| Source dataset | uspto-grants-2012_10 |
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| ORD ID | ord-780925deed874470bc1486e367ebd867 |
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| Source note | uspto-grants-2012_10 |
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