Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2060321Generated: October 31, 2026

3-Chlorobenzaldehyde → HCID 57924044, compound

https://huagongshe.com/reaction/2060321

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-ChlorobenzaldehydeHCID 11477—
Reactant1H-Imidazole-1-propanamineHCID 78736—
ReactantEthyl 2-oxooctanoateHCID 10888659—
SolventEthanolHCID 702—
ProductHCID 57924044HCID 57924044—

Reaction Conditions

Temperature50 °C

Reaction Steps

3-Imidazol-1-yl-propylamine (1 mmol) and 3-Chloro-benzaldehyde (1 mmol) were added to ethanol (5 ml). After 30 min 2-Oxo-octanoic acid ethyl ester (1 mmol) was added. The reaction was heated to 50° C. and stirred for 24 h. After evaporation of the solvent the residue was purified with chromatographic methods.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08278345B2
Source datasetuspto-grants-2012_10
ORD IDord-f42637c480ec48088116219a3f0c35f6
Source noteuspto-grants-2012_10