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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2060332Generated: November 2, 2026

3,4-Dichlorobenzaldehyde → HCID 178519911, compound

https://huagongshe.com/reaction/2060332

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,4-DichlorobenzaldehydeHCID 22710—
ReactantEthyl 4-cyclohexyl-2,4-dioxobutanoateHCID 23005470—
ReactantHCID 178507353HCID 178507353—
SolventEthanolHCID 702—
ProductHCID 178519911HCID 178519911—

Reaction Conditions

Temperature50 °C

Reaction Steps

1H-Benzoimidazol-5-ylamine (1 mmol) and 3,4 Dichlorobenzaldehyde (1 mmol) were added to ethanol (5 ml). After 30 min 4-Cyclohexyl-2,4-dioxo-butyric acid ethyl ester (1 mmol) was added. The reaction was heated to 50° C. and stirred for 24 h. After evaporation of the solvent the residue was purified with chromatographic methods.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08278345B2
Source datasetuspto-grants-2012_10
ORD IDord-bea395cb470c4b08a48d79213d32cf9a
Source noteuspto-grants-2012_10