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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2060334Generated: October 31, 2026

4-Pyridin-2-ylbenzaldehyde → HCID 178450347, compound

https://huagongshe.com/reaction/2060334

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Pyridin-2-ylbenzaldehydeHCID 1515240—
ReactantEthyl 2,4-dioxoheptanoateHCID 3006750—
ReactantHCID 178507353HCID 178507353—
SolventEthanolHCID 702—
ProductHCID 178450347HCID 178450347—

Reaction Conditions

Temperature50 °C

Reaction Steps

1H-Benzoimidazol-5-ylamine (1 mmol) and 4-Pyridin-2-yl-benzaldehyde (1 mmol) were added to ethanol (5 ml). After 30 min 2,4-Dioxo-heptanoic acid ethyl ester (1 mmol) was added. The reaction was heated to 50° C. and stirred for 24 h. After evaporation of the solvent the residue was purified with chromatographic methods.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08278345B2
Source datasetuspto-grants-2012_10
ORD IDord-fe1ff434d8224be6a802a5c2f08a19fd
Source noteuspto-grants-2012_10