Acetone → HCID 58335259, compound

Participants

Reaction Steps

The title compound was prepared as described in Example 15, Step 3 using 4-bromo-1-(diethoxymethyl)-2-fluorobenzene (2.8 g, 0.01 mol), n-BuLi (4.8 mL of 2.5M, 0.012 mol), and acetone (0.96 mL, 0.013 mol) as starting materials. 1H NMR (400 MHz, CDCl3): δ 10.23 (s, 1H), 7.47 (d, 1H), 7.26 (s, 1H), 7.28 (d, 1H), 5.74 (s, 1H), 3.62 (s, 2H), 3.47-3.52 (m, 2H), 1.48 (s, 6H), 1.16 (t, 6H).

Provenance & Evidence