Indole → HCID 59239027, compound

Participants

Reaction Steps

The title compound was prepared in a manner analogous to Example 28 except the starting indole is 5,7-diBOC-2,10-dichloro-6-hydroxyindolo[2,3-b]carbazole and the reagent is 6-dimethylamino-1-hexanol. 1H-NMR (400 MHz, CDCl3) δ ppm 8.35 (s, 1H), 8.20 (s, 2H), 8.08 (s, 2H), 7.41-7.32 (m, 4H), 4.28 (t, J=6.4 Hz, 2H), 2.31 (t, J=7.2 Hz, 2H), 2.23 (s, 6H), 2.00-1.90 (m, 2H), 1.65-1.42 (m, 6H); MS (ESI) m/z 466.2 (M−H)−; MS (ESI) m/z 468.1 (M+H)+

Provenance & Evidence