HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indole → HCID 59238876, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indole | HCID 798 | — |
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 68651246 | HCID 68651246 | — |
| Product | HCID 59238876 | HCID 59238876 | — |
Reaction Steps
The title compound was prepared in a manner analogous to Example 70 except the starting indole is 5,7-diBOC-2,10-dibromo-6-(4-bromobutoxy)indolo[2,3-b]carbazole and the reagent is morpholine. 1H-NMR (400 MHz, DMSO-d6) δ ppm 11.22 (s, 2H), 8.64 (s, 1H), 8.25 (d, J=1.6 Hz, 2H), 7.44 (dd, J=8.4, 2.0 Hz, 2H), 7.41 (d, J=8.4 Hz, 2H), 4.26 (t, J=6.8 Hz, 2H), 3.57-3.40 (m, 6H), 2.32-2.18 (m, 4H), 1.92-1.80 (m, 2H), 1.65-1.50 (m, 2H); MS (ESI) m/z 570.0 (M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08278341B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-f8dceaf3f19945db8151cebdeb72b5ed |
| Source note | uspto-grants-2012_10 |