Thiophenol → HCID 67545329, compound

Participants

Reaction Steps

To a solution of 201 mg of phenyl 3,N-diphenylpropynimidothioate in 5 ml of THF was added 0.08 ml of thiophenol and tert-butoxy potassium (a catalytic amount). The mixture was stirred at room temperature for 2 hours and then refluxed for 2 hours. The reaction mixture was concentrated under vacuum. The residue was purified by medium pressure preparative HPLC to obtain 269 mg of phenyl 3,N-diphenyl-3-(phenylthio)-2-propenimidothioate (hereinafter referred to as the present compound 42) as a yellow oil.

Provenance & Evidence