HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen chloride-ethyl acetate → HCID 68421306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 86594134 | HCID 86594134 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 68421306 | HCID 68421306 | — |
Reaction Steps
1.40 g (2.57 mmol) of the compound obtained in step 1 described above was dissolved in 12 ml of ethyl acetate. 10 ml of 4 N hydrochloric acid/ethyl acetate was added to the obtained solution under cooling with ice. The temperature was gradually elevated to room temperature. After stirring for 3.5 hours, the solvent was evaporated under reduced pressure to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08278329B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-43ed084719f645978a20e91366289737 |
| Source note | uspto-grants-2012_10 |