HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → Phenacyltetrahydrothiophenium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Tetrahydrothiophene | HCID 1127 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Solvent | Nitromethane | HCID 6375 | — |
| Product | Phenacyltetrahydrothiophenium bromide | HCID 11346720 | — |
Reaction Steps
Phenacyl bromide (88.2 g, 0.44 mole) and 39.1 g (0.44 mole) of tetrahydrothiophene were dissolved in 220 g of nitromethane, and they were stirred at room temperature for 4 hours. Into the reaction solution were added 800 g of water and 400 g of diethyl ether, and the separated water layer was taken to obtain the aqueous solution of the intended phenacyl tetrahydrothiophenium bromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08283104B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-48dfd8a72a224fcf9c116d359c3b4160 |
| Source note | uspto-grants-2012_10 |