HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichlone → 1,4-Naphthalenedione, 2-chloro-3-[cis-4-(4-chlorophenyl)cyclohexyl]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichlone | HCID 8342 | — |
| Reactant | Ammonium Persulfate | HCID 62648 | — |
| Reactant | HCID 178525693 | HCID 178525693 | — |
| Catalyst | Silver Nitrate | HCID 24470 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 1,4-Naphthalenedione, 2-chloro-3-[cis-4-(4-chlorophenyl)cyclohexyl]- | HCID 11101070 | — |
Reaction Steps
condensing 2,3-dichloro-1,4-naphthoquinone of formula (3) with trans 4-(4-chlorophenyl)cyclohexane-1-carboxylic acid of formula (4) in acetonitrile in presence of silver nitrate and ammonium persulfate in a suitable solvent to provide 2-[4-(4-chlorophenyl)cyclohexyl]-3-chloro-1,4-naphthoquinone of formula (5);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08283499B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-102d2885fc924575a36ac085eb045922 |
| Source note | uspto-grants-2012_10 |