HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-Methoxy-6-methylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Methoxy-6-methylbenzoic acid | HCID 273170 | — |
| Product | 2-Methoxy-6-methylbenzoyl chloride | HCID 12892675 | — |
Reaction Steps
2-Methoxy-6-methyl-benzoic acid (21.4 g, 0.129 mol) was refluxed for 3 hours in 230 mL thionyl chloride. Excess thionyl chloride was removed under reduced pressure. Co-evaporation of the residue with toluene gave 23.8 g of 2-methoxy-6-methyl-benzoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08283354B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-9fd994dbf3654383af256f0498fa89a2 |
| Source note | uspto-grants-2012_10 |