(2R,3S,4R,5R,6S)-2-[(2R,3S,4S,5S)-2,5-bis(chloromethyl)-3,4-dihydroxyoxolan-2-yl]oxy-5-chloro-6-(hydroxymethyl)oxane-3,4-diol → ethyl lauroyl arginine HCL

Participants

Reaction Steps

A series of films containing varying amounts of the arginine derivative compound they hydrochloride salt of ethyl lauroyl arginine designated Compositions A, B and C were prepared by using the ingredients listed in Table VI below. In preparing the film, the hydroxyl propylmethylcellulose polymer ingredient (Methocel E5LV) and carrageenan as added at a temperature of 70° C. to 90° C., to half the amount of total deionized water used, and the solution stirred for 20 minutes at a slow speed using IKA Labortechnik Model RW20DZMixer. The remaining amount of water maintained at room temperature (21° C.) was then added and the mixing continued for 40 minutes. To this solution was added the corn starch ingredient (Cerestar Polar Tex Instant 12640) and the mixture stirred for an additional 20 minutes until the starch was completely dispersed and a homogenous mixture was formed. To this mixture was added sucralose and mixed for 10 minutes after which the emulsifier Tween 80 was added and mixed for an additional 5 minutes. Thereafter, flavor was thoroughly mixed for an additional 30 minutes to form a flurry emulsion to which as a final step the hydrochloride salt of ethyl lauroyl arginine HCL (ELAH) dispersed in canola oil was slowly added until evenly dispersed in the film ingredient slurry. The emulsion was then cast on a polyethylene coated paper substrate and dried in a convection oven at 110° C. to form a solid thin (30 to 60 μm thick) film.

Provenance & Evidence