HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66893177, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59366192 | HCID 59366192 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66893177 | HCID 66893177 | — |
Reaction Steps
300 mg of 4-(2,4-dimethoxyphenyl)-[1,4]diazepane-1-carboxylic acid tert-butyl ester was dissolved in 10 mL of 4 N HCl in dioxane. The mixture was stirred at room temperature for 2 hrs and evaporated to dryness to give the desired product (270 mg) as a hydrochloride salt. MS (ES) m/z 237.2 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288373B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-5bfc9294b569482a847a6b36b6df98de |
| Source note | uspto-grants-2012_10 |