化工社化工社 化学情報印刷レポート · 研究参考用
p-Methylpropiophenone → N-(2-Methyl-6-phenyl-pyrimidin-4-yl)-N'-[1-p-tolyl-propylidene]-hydrazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | p-Methylpropiophenone | HCID 21429 | — |
| 反応物 | 4-Hydrazinyl-2-methyl-6-phenylpyrimidine | HCID 824627 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | N-(2-Methyl-6-phenyl-pyrimidin-4-yl)-N'-[1-p-tolyl-propylidene]-hydrazine | HCID 73320072 | — |
反応手順
The title compound was prepared from 4-hydrazino-2-methyl-6-phenylpyrimidine (300 mg, 1.5 mmol) and 1-p-Tolyl-propan-1-one (174 μL, 1.05 mmol) in 3.0 mL of ethanol by a procedure similar to example 1, step 4 yielding 110 mg (22%) of a white solid. HPLC Purity: 96%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08288398B2 |
| 出典データセット | uspto-grants-2012_10 |
| ORD ID | ord-a4909e30ae9c4eb38b3b8ef8437c01bc |
| 出典メモ | uspto-grants-2012_10 |