m,alpha-Dichlorotoluene → 1-(3-chlorobenzyl)-1H-1,2,4-triazol-3-amine

HRID 2063634Notes

Reaction equation

HRID 2063634 reaction equation
[NH2:1][C:2]1[N:6]=[CH:5][NH:4][N:3]=1.[Cl:7][C:8]1[CH:9]=[C:10]([CH:13]=[CH:14][CH:15]=1)[CH2:11]Cl>>[Cl:7][C:8]1[CH:9]=[C:10]([CH:13]=[CH:14][CH:15]=1)[CH2:11][N:4]1[CH:5]=[N:6][C:2]([NH2:1])=[N:3]1

Participants

3

Reactant 2

HCID 12103m,alpha-DichlorotolueneHCID 178418311HCID 178418311, compound

Product 1

HCID 70193361-(3-chlorobenzyl)-1H-1,2,4-triazol-3-amine

Procedure

Prepared in analogy to example 3a) starting with 3-amino-1,2,4-triazole and 3-chloro benzyl chloride. The title compound was obtained as a colorless solid (Yield=9%). MS ISP (m/e): 211.0 & 209.0 (43 & 100) [M+].

Workup

  1. customPrepared in analogy to example 3a)

Sources & evidence

ORD record
ord-c7b3d71246f34d39896b0eff38c3214e
Source dataset
uspto-grants-2012_10
Patent number
US08288403B2

Reaction notes

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