(1-Bromoethyl)benzene → HCID 64120767, compound

HRID 2063646Notes

Reaction equation

HRID 2063646 reaction equation
[NH2:1][C:2]1[N:6]=[CH:5][NH:4][N:3]=1.Br[CH:8]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)[CH3:9]>>[C:10]1([CH:8]([N:4]2[CH:5]=[N:6][C:2]([NH2:1])=[N:3]2)[CH3:9])[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 11454(1-Bromoethyl)benzeneHCID 178418311HCID 178418311, compound

Product 1

HCID 64120767HCID 64120767, compound

Procedure

Prepared in analogy to example 3a) starting with 3-amino-1,2,4-triazole and (1-bromoethyl)benzene. The title compound was obtained as a colorless solid (Yield=10%). MS ISP (m/e): 189.2.0 (100) [(M+H)+].

Workup

  1. customPrepared in analogy to example 3a)

Sources & evidence

ORD record
ord-828925f768954013815129fb5ed054ca
Source dataset
uspto-grants-2012_10
Patent number
US08288403B2

Reaction notes

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