3,4,5-Trifluorobenzyl bromide → HCID 67343001, compound

HRID 2063650Notes

Reaction equation

HRID 2063650 reaction equation
[NH2:1][C:2]1[N:6]=[CH:5][NH:4][N:3]=1.[F:7][C:8]1[CH:9]=[C:10]([CH:13]=[C:14]([F:17])[C:15]=1[F:16])[CH2:11]Br>>[F:7][C:8]1[CH:9]=[C:10]([CH:13]=[C:14]([F:17])[C:15]=1[F:16])[CH2:11][N:4]1[CH:5]=[N:6][C:2]([NH2:1])=[N:3]1

Participants

3

Reactant 2

HCID 27770623,4,5-Trifluorobenzyl bromideHCID 178418311HCID 178418311, compound

Product 1

HCID 67343001HCID 67343001, compound

Procedure

Prepared in analogy to example 3a) starting with 3-amino-1,2,4-triazole and 3,4,5-trifluorobenzyl bromide. A pure fraction of the title compound was obtained as a colorless solid (Yield=4%). MS ISP (m/e): 229.2 (100) [(M+H)+].

Workup

  1. customPrepared in analogy to example 3a)

Sources & evidence

ORD record
ord-9cb42db025744727be8f7332a4398190
Source dataset
uspto-grants-2012_10
Patent number
US08288403B2

Reaction notes

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