Methyl 3-(bromomethyl)benzoate → HCID 67378047, compound

HRID 2063680Notes

Reaction equation

HRID 2063680 reaction equation
[NH2:1][C:2]1[N:6]=[CH:5][NH:4][N:3]=1.[CH3:7][O:8][C:9](=[O:18])[C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([CH2:16]Br)[CH:11]=1>>[CH3:7][O:8][C:9](=[O:18])[C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([CH2:16][N:4]2[CH:5]=[N:6][C:2]([NH2:1])=[N:3]2)[CH:11]=1

Participants

3

Reactant 2

HCID 517981Methyl 3-(bromomethyl)benzoateHCID 178418311HCID 178418311, compound

Product 1

HCID 67378047HCID 67378047, compound

Procedure

Prepared in analogy to example 3a) starting with 3-amino-1,2,4-triazole and methyl-3-(bromomethyl)benzoate. The title compound was obtained as a colorless solid (Yield=8%). MS ISP (m/e): 233.1 (100) [(M+H)+].

Workup

  1. customPrepared in analogy to example 3a)

Sources & evidence

ORD record
ord-933a6a6111814659a49582749bf79de8
Source dataset
uspto-grants-2012_10
Patent number
US08288403B2

Reaction notes

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