HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenepropanal → 2-Bromo-3-phenylpropanal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenepropanal | HCID 7707 | — |
| Reactant | Bromine | HCID 24408 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Bromo-3-phenylpropanal | HCID 11390228 | 143.6% |
Reaction Steps
To a solution of 3-phenylpropionaldehyde (13.4 g, purity 90%, 0.09 mol) in dichloromethane at 0° C. was slowly added bromine (13.7 g, 0.085 mol). After 12 h at rt the solvent was evaporated to yield crude title compound (26.0 g (purity about 60%), 81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288403B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-0f64e52a1a4748c8a4bf3b5011774cc0 |
| Source note | uspto-grants-2012_10 |