HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Methoxyphenyl)morpholine → HCID 66760147, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Methoxyphenyl)morpholine | HCID 3759546 | — |
| Reactant | 5-bromo-2,2,6,7-tetramethyl-1-benzofuran-3(2H)-one | HCID 66759713 | — |
| Product | HCID 66760147 | HCID 66760147 | 34.1% |
Reaction Steps
By using 5-bromo-2,2,6,7-tetramethyl-1-benzofuran-3(2H)-one (488 mg, 1.72 mmol) synthesized in Reference Example 18 and 2-(4-methoxyphenyl)morpholine (500 mg, 2.59 mmol), the reaction was carried out in the same manner as Reference Example 59 to synthesize 224 mg of the title compound (yield 34%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288390B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-8e0aee09807941559d800f565e602e7c |
| Source note | uspto-grants-2012_10 |