HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-methoxypyridine → HCID 59485049, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-methoxypyridine | HCID 2734895 | — |
| Reactant | 1-(2,2,4,6,7-Pentamethyl-2,3-dihydro-1-benzofuran-5-yl)piperazine | HCID 66759731 | — |
| Product | HCID 59485049 | HCID 59485049 | 37.3% |
Reaction Steps
By using 1-(2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-yl)piperazine (210 mg, 0.765 mmol) synthesized in Reference example 61 and 5-bromo-2-methoxypyridine (216 mg, 1.15 mmol), the reaction was carried out in the same manner as Example 23 to synthesize the title compound 109 mg (yield 37%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288390B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-6ea93b66ef5a49d7a990ecf18b6817f8 |
| Source note | uspto-grants-2012_10 |