HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(p-Tolyl)piperazine → HCID 59485099, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(p-Tolyl)piperazine | HCID 83113 | — |
| Reactant | HCID 66760475 | HCID 66760475 | — |
| Product | HCID 59485099 | HCID 59485099 | 42% |
Reaction Steps
By using 5-bromo-7-methoxy-2,4,6-trimethyl-2,3-dihydro-1-benzofuran (542 mg, 2.0 mmol) synthesized in Reference example 83 and 1-(4-methylphenyl)piperazine (704 mg, 4.0 mmol), the reaction was carried out in the same manner as Example 21 to synthesize the title compound 306 mg (yield 42%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288390B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-5423e6e6bdd346ff8caf02cab3533e4d |
| Source note | uspto-grants-2012_10 |