HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromophenetole → HCID 59485044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromophenetole | HCID 68523 | — |
| Reactant | HCID 66759462 | HCID 66759462 | — |
| Product | HCID 59485044 | HCID 59485044 | 33.4% |
Reaction Steps
By using 1-(7-methoxy-2,4,6-trimethyl-2,3-dihydro-1-benzofuran-5-yl)piperazine (552 mg, 2.0 mmol) synthesized in Reference example 88 and 1-bromo-4-ethoxybenzene (804 mg, 4.0 mmol), the reaction was carried out in the same manner as Example 23 to synthesize the title compound 265 mg (yield 33%). Melting point was 117 to 119° C. (ethanol-water).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288390B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-6fccf7e6eff84e68938f400e7478a3e1 |
| Source note | uspto-grants-2012_10 |