HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Anisidine → HCID 59485095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Anisidine | HCID 7732 | — |
| Reactant | HCID 66760461 | HCID 66760461 | — |
| Product | HCID 59485095 | HCID 59485095 | 25% |
Reaction Steps
By using 6-bromo-N,N-bis(2-chloroethyl)-2,2,4,7-tetramethyl-2,3-dihydro-1-benzofuran-5-amine (492 mg, 1.25 mmol) synthesized in Reference Example 152 and 4-methoxyaniline (185 mg, 1.50 mmol), the reaction was carried out in the same manner as Example 117 to synthesize 138 mg of the title compound (yield 25%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288390B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-59125125a26f41a292dde8f4c22d9137 |
| Source note | uspto-grants-2012_10 |