Lithium Hydroxide → HCID 67364661, compound

Participants

Reaction Steps

Dissolve the compound obtained in Step A (1.26×10−3 mol) in a mixture of acetonitrile (45 ml) and water (9 ml). Add lithium hydroxide (1.26×10−2 mol) and heat at 50° C. with stirring. After heating for 5 hours and 30 minutes, the dark-brown reaction mixture is poured into water (100 ml). Extract 3 times with ethyl acetate (50 ml). The organic phase is then washed with water and then with brine, dried over magnesium sulphate, filtered and evaporated to dryness under reduced pressure.

Provenance & Evidence