Cyclohexanemethylamine → HCID 178522794, compound

HRID 2064575Notes

Reaction equation

HRID 2064575 reaction equation
[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]([C:10]2[NH:14][C:13]3[CH:15]=[CH:16][C:17]([C:19](O)=[O:20])=[CH:18][C:12]=3[N:11]=2)=[N:2]1.[CH:22]1([CH2:28][NH2:29])[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23]1>>[CH:22]1([CH2:28][NH:29][C:19]([C:17]2[CH:16]=[CH:15][C:13]3[NH:14][C:10]([C:3]4[C:4]5[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=5)[NH:1][N:2]=4)=[N:11][C:12]=3[CH:18]=2)=[O:20])[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23]1

Participants

3

Reactant 2

HCID 76688CyclohexanemethylamineHCID 178524162HCID 178524162, compound

Product 1

HCID 178522794HCID 178522794, compound

Procedure

Starting with 20 mg of 2-(1H-indazol-3-yl)-1H-benzimidazole-5-carboxylic acid and 18.7 ml of cyclohexylmethylamine, 16.1 mg of 2-(1H-indazol-3-yl)-1H-benzimidazole-5-carboxylic acid N-cyclohexylmethyl)amide are obtained in the form of a white powder.

Workup

  1. customare obtained in the form of a white powder

Sources & evidence

ORD record
ord-4e008ac0c5904848ae122cd4f1183f2d
Source dataset
uspto-grants-2012_10
Patent number
US08288425B2

Reaction notes

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