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HRID2064796

反应详情

EQUATION

反应方程式

HRID 2064796 的结构方程式

REACTANTS

反应物

2
结构：Cc1noc(C)c1C(=O)O
HCID75636

3,5-Dimethylisoxazole-4-carboxylic acid

C6H7NO3

结构：CC(C)(C)OC(=O)N1[C@H](CN)C[C@@H]2C[C@@H]21
HCID58278675

未命名化合物

PRODUCTS

生成物

1
结构：Cc1noc(C)c1C(=O)NC[C@@H]1C[C@@H]2C[C@@H]2N1C(=O)OC(C)(C)C
HCID67081394

未命名化合物

PROCEDURE

实验过程

prepared by reaction of (1S,3S,5S)-3-aminomethyl-2-aza-bicyclo[3.1.0]hexane-2-carboxylic acid tert-butyl ester with 3,5-dimethyl-isoxazole-4-carboxylic acid. LC-MS (acidic): tR=0.93 min; [M+H]+=336.2. 1H-NMR (CDCl3): δ=0.51 (bs, 1H); 0.81-0.87 (m, 1H); 1.49 (s, 9H); 1.50-1.56 (m, 1H); 1.74 (bd, J=13.5 Hz, 1H); 2.47 (s, 3H); 2.52-2.62 (m, 1H); 2.64 (s, 3H); 3.05-3.11 (m, 1H); 3.57-3.65 (m, 2H); 4.32-4.40 (m, 1H); 7.95 (bs, 1H).