o-Methylcinnamic acid → HCID 66929214, compound

HRID 2065170Notes

Reaction equation

HRID 2065170 reaction equation
[CH3:1][C:2]1([CH2:7][CH2:8][CH2:9][CH2:10][N:11]2[CH:15]=[C:14]([NH2:16])[CH:13]=[N:12]2)[O:6]CCO1.[C:17]1([CH3:28])[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1/[CH:23]=[CH:24]/[C:25](O)=[O:26]>>[O:6]=[C:2]([CH3:1])[CH2:7][CH2:8][CH2:9][CH2:10][N:11]1[CH:15]=[C:14]([NH:16][C:25](=[O:26])/[CH:24]=[CH:23]/[C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][C:17]=2[CH3:28])[CH:13]=[N:12]1

Participants

3

Reactant 2

HCID 819020o-Methylcinnamic acidHCID 669287261-[4-(2-Methyl-[1,3]dioxolan-2-yl)-butyl]-1H-pyrazol-4-ylamine

Product 1

HCID 66929214HCID 66929214, compound

Procedure

Following general procedure B followed by either C or D, starting from 1-[4-(2-methyl-[1,3]dioxolan-2-yl)-butyl]-1H-pyrazol-4-ylamine and (E)-3-o-tolyl-acrylic acid.

Sources & evidence

ORD record
ord-d79deb6c2dcf48789e2fc05a5ca57f90
Source dataset
uspto-grants-2012_10
Patent number
US08288419B2

Reaction notes

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