(2E)-3-(2,4-Dimethoxyphenyl)-2-propenoic acid → HCID 66928976, compound

HRID 2065260Notes

Reaction equation

HRID 2065260 reaction equation
[CH3:1][C:2]1([C:7]2[O:11][C:10]([CH2:12][N:13]3[CH:17]=[CH:16][C:15]([NH2:18])=[N:14]3)=[CH:9][CH:8]=2)[O:6]CCO1.[CH3:19][O:20][C:21]1[CH:26]=[C:25]([O:27][CH3:28])[CH:24]=[CH:23][C:22]=1/[CH:29]=[CH:30]/[C:31](O)=[O:32]>>[C:2]([C:7]1[O:11][C:10]([CH2:12][N:13]2[CH:17]=[CH:16][C:15]([NH:18][C:31](=[O:32])/[CH:30]=[CH:29]/[C:22]3[CH:23]=[CH:24][C:25]([O:27][CH3:28])=[CH:26][C:21]=3[O:20][CH3:19])=[N:14]2)=[CH:9][CH:8]=1)(=[O:6])[CH3:1]

Participants

3

Reactant 2

HCID 734009(2E)-3-(2,4-Dimethoxyphenyl)-2-propenoic acidHCID 669287811-[5-(2-Methyl-[1,3]dioxolan-2-yl)-furan-2-ylmethyl]-1H-pyrazol-3-ylamine

Product 1

HCID 66928976HCID 66928976, compound

Procedure

Following general procedure B followed by T, starting from 1-[5-(2-methyl-[1,3]dioxolan-2-yl)-furan-2-ylmethyl]-1H-pyrazol-3-ylamine and (E)-3-(2,4-dimethoxy-phenyl)-acrylic acid. LC-MS-conditions 05b: tR=0.97 min; [M+H]+=396.15.

Sources & evidence

ORD record
ord-cdd95ae3c1f14de6935c43207ec47c89
Source dataset
uspto-grants-2012_10
Patent number
US08288419B2

Reaction notes

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